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When there is no specific experience in the field, processes using dense phase fluids are generally approached by starting with feasibility studies at laboratory level, simulating the processes with minimal amounts of product. If the tests are successful, that is to say, if they confirm the generic applicability of subcritical or supercritical C02 to a given
treatment, suggesting possible development on an industrial scale, it is necessary to perform a further test with larger volumes of product.
Pilot plants allow to confirm that laboratory results are reproducible when more significant quantities are involved and accordingly allow to determine the critical variables, the timings, the yield and other operating parameters involved in planning a scale-up to the industrial level.
This family of plants includes machines capable of processing volumes typically between 1 and 25 I. These machines are highly flexible because they must allow to evaluate various operating possibilities and test several alternatives during the study and optimization of the process. A second scale-up is often required before defining an industrial plant if the matrices to be processed are very expensive.
Refining processes in these plants is obviously highly critical. This is the stage when it becomes clear whether a process can be industrially utilized, with the consequent economic implications. Sometimes, the user's organization has the expertise required to optimize the processes but cannot install such plants.
In other cases, for understandable confidentiality reasons, there is no wish to leak valuable information which might help other companies in the same development. Fedegari Autoclavi SpA is able to meet any requirement, either directly or by means of its partners, with a wide range of offers: from the leasing
of extremely flexible pilot plants to the conduction of tests with the backing of an analysis laboratory to the supply of customized plants of the chosen size. In the case of processes for which transfer of the matrices to be processed is troublesome, some plants can be easily shipped to the user's site.
Although these plants are meant to perform tests, they are equipped with all the appropriate safety devices and offer a far higher degree of flexibility than industrial plants, which are designed for a far narrower range of applications.






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